PENAPISAN FITOKIMIA DAN ISOLASI SENYAWA TRITERPENOID DARI FRAKSI ETIL ASETAT KULIT BATANG KECAPI (S andoricum koetjape)

ARDIAN S, NIZAR and Eliza, Eliza and Ferlinahayati, Ferlinahayati (2018) PENAPISAN FITOKIMIA DAN ISOLASI SENYAWA TRITERPENOID DARI FRAKSI ETIL ASETAT KULIT BATANG KECAPI (S andoricum koetjape). Undergraduate thesis, Sriwijaya University.

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Abstract

Phytochemical test of Sandoricum koetjapefollowed by isolation triterpenoid compound from ethyl acetate fraction from S. koetjapestem bark have been done. The isolation process was carried out through the extraction step by maceration method and separation of compound and purification by liquid partition and chromatography methods. The purity test was carried out by thin-layer chromatography test using three eluent mixed systems and also using melting point test and characterization of compound using infrared spectroscopy, 1H-NMR, 13C-NMR, HSQC, and HMBC. Phytochemical test result showed that S. koetjapecontain flavonoid, saponin, steroid, and triterpenoid. The isolation result was obtained pure compound in the form of white crystalline solid with melting point 235-237oC. The purity test showed consistanly one spot with a mixture hexane: ethyl acetate (8:2) with Rf 0.625; hexane: chloroform (3:7) with Rf0.375; hexane:acetone (8:2) with Rf0.625 based on the analysis of Infrared spectra data, 1H-NMR, 13C-NMR, HSQC, and HMBC, it can be concluded that the isolated compound is a group tritepenoids compound of oleanan origin of briononicacid.

Item Type:	Thesis (Undergraduate)
Uncontrolled Keywords:	Stem bark kecapi (S. koetjape), triterpenoid, briononic acid, phytochemical test.
Subjects:	Q Science > QD Chemistry > QD1-999 Chemistry Q Science > QD Chemistry > QD450-801 Physical and theoretical chemistry
Divisions:	08-Faculty of Mathematics and Natural Science > 47201-Chemistry (S1)
Depositing User:	Mrs Dies Meirita Sari
Date Deposited:	30 Jul 2019 02:03
Last Modified:	30 Jul 2019 02:03
URI:	http://repository.unsri.ac.id/id/eprint/1222

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