Synthesis of Tris(4-Methoxyphenyl)Phenylsilane Using Phenylsilane and 4-Iodo Anisole Catalyzed by Palladium Complex

Lesbani, Aldes and Mohadi, Risfidian and Eliza, Eliza and Mardiyanto, Mardiyanto Synthesis of Tris(4-Methoxyphenyl)Phenylsilane Using Phenylsilane and 4-Iodo Anisole Catalyzed by Palladium Complex. Makara Seri Science.

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Abstract

The synthesis of tris(4-methoxyphenyl)phenylsilan through the coupling reaction of phenylsilane and 4-iodoanisole using palladium tertiary tributylphosphine as a catalyst was carried out through the determination of the base, solvent, and reaction time. The results showed that tris(4-methoxyphenyl)phenylsilane can be synthesized to form maximum yield using 1,4-diazabicyclo2,2,2octane (DABCO) as a base, tetrahydrofuran as a solvent, and a 5-day reaction time. The highest yield of tris(4-methoxyphenyl)phenylsilane was 35\%.

Item Type: Article
Subjects: Q Science > QD Chemistry > QD1-999 Chemistry
Divisions: 08-Faculty of Mathematics and Natural Science > 47201-Chemistry (S1)
Depositing User: Mr Aldes Lesbani
Date Deposited: 13 Dec 2019 07:24
Last Modified: 27 Jun 2024 07:54
URI: http://repository.unsri.ac.id/id/eprint/21588

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