Lesbani, Aldes and Mohadi, Risfidian and Eliza, Eliza and Mardiyanto, Mardiyanto Synthesis of Tris(4-Methoxyphenyl)Phenylsilane Using Phenylsilane and 4-Iodo Anisole Catalyzed by Palladium Complex. Makara Seri Science.
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Abstract
The synthesis of tris(4-methoxyphenyl)phenylsilan through the coupling reaction of phenylsilane and 4-iodoanisole using palladium tertiary tributylphosphine as a catalyst was carried out through the determination of the base, solvent, and reaction time. The results showed that tris(4-methoxyphenyl)phenylsilane can be synthesized to form maximum yield using 1,4-diazabicyclo2,2,2octane (DABCO) as a base, tetrahydrofuran as a solvent, and a 5-day reaction time. The highest yield of tris(4-methoxyphenyl)phenylsilane was 35\%.
| Item Type: | Article |
|---|---|
| Subjects: | Q Science > QD Chemistry > QD1-999 Chemistry |
| Divisions: | 08-Faculty of Mathematics and Natural Science > 47201-Chemistry (S1) |
| Depositing User: | Mr Aldes Lesbani |
| Date Deposited: | 13 Dec 2019 07:24 |
| Last Modified: | 13 Dec 2019 07:24 |
| URI: | http://repository.unsri.ac.id/id/eprint/21588 |
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