Korespondensi Characterization Porous HA/SiO2 Composite Prepared Using Natural Space Holder

Gunawan, Gunawan (2023) Korespondensi Characterization Porous HA/SiO2 Composite Prepared Using Natural Space Holder. FT. Unsri.

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Abstract

Hydroxyapatite based on bovine bone has been developed in addition to medical needs, adsorbents, catalysts, and other engineering applications. The use of hydroxy apatite-based catalysts in the industry is still very high, one of which is solid catalysts. This study aims to develop a solid porous catalyst from a HA/Si0, composite. The porous composite was prepared with Si0 as much as 25% of the total weight fraction and utilized sweet potato powder heated at a temperature of 150C as a space holder. The manufacturing process begins by mixing hydroxyapatite powder (200 pm), Si0 powder (200 pm), and purple sweet potato powder (200 pm), then mixing it using a ball mill with a rotating speed of 225 rpm for I h. The mixture was then put into the molding and compacted with a pressure of 69.805 MPa. The green body was then sintered at I I 00 and 1200 °C and held for 3 h. Apparent density measurements were carried out using the Archimedes method, and the highest density was 1.4983 g/cm' with a porosity of 50.34% in the 30% space holder specimen. The XRD test shows that the dominant phases are hydroxy apatite (HA), 8-TCP, and Si0. The compressive strength test showed the highest average compressive strength of 33,073 MPa in the 30% space holder specimen. The SEM observations showed pores formed in the samples with varying sizes ranging from 4.510 to 67 .32 µm and showed interconnecting porous.

Item Type:	Other
Subjects:	#3 Repository of Lecturer Academic Credit Systems (TPAK) > Corresponding Author
Divisions:	03-Faculty of Engineering > 21201-Mechanical Engineering (S1)
Depositing User:	S.T., M.T. Gunawan Gunawan
Date Deposited:	05 May 2023 07:42
Last Modified:	05 May 2023 07:42
URI:	http://repository.unsri.ac.id/id/eprint/99583

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