STUDI KONVERSI SIKLOHEKSANON MENJADI ASAM ADIPAT DENGAN KATALIS SENYAWA POLIOKSOMETALAT

FITRILIANA, FITRILIANA and Lesbani, Aldes and Mohadi, Risfidian (2013) STUDI KONVERSI SIKLOHEKSANON MENJADI ASAM ADIPAT DENGAN KATALIS SENYAWA POLIOKSOMETALAT. Undergraduate thesis, Sriwijaya University.

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Abstract

Conversion of cyclohexanone to adipic acid using 30% H2O2 is an ideal clean oxidant H5BW12O40 and H4PVM011O40 as catalysts has been done. The influence of reaction time and temperature oxidation reaction studied of reaction time 6-9 hours and temperature 80°C-105°C. The conversion of adipic acid was characterized by measuring the melting point, identification using GC-MS, spectrophotometer FT-IR and spectrometer NMR (13C and 1H). The results showed that adipic acid is formed from oxidation of cyclohexanone yielded 30% - 48% with melting point in the range of 149°C-151°C. The effect of reaction time gave adipic acid 41% for reaction time 7 hours. The effect of temperature oxidation reaction showed the highest adipic acid obtained at 100°C yielded 48%. The use of H4PVM011O40 did not produced adipic acid. The FT-IR spectra of the product is well agreed with the FT-IR spectra of adipic acid Standard and NMR spectra (13C and 1H)NMR showed that adipic acid have a formula C6H10O4 is agreed with molecular structure of adipic acid.

Item Type:	Thesis (Undergraduate)
Uncontrolled Keywords:	adipic acid, cyclohexanone, hydrogen peroxide, catalysts.
Subjects:	Q Science > QD Chemistry > QD146-197 Inorganic chemistry
Divisions:	08-Faculty of Mathematics and Natural Science > 47201-Chemistry (S1)
Depositing User:	Mrs Furika Furika
Date Deposited:	18 Mar 2022 06:33
Last Modified:	18 Mar 2022 06:33
URI:	http://repository.unsri.ac.id/id/eprint/66289

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